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Polaris

Polaris investigates local and/or long-range structures of crystalline materials over a wide range of temperatures and pressures, with academic and applied impact. A large detector array allows fast data collection or the use of very small samples. Recent highlights include studies of lithium-ion batteries, high-performance alloys, and salty ices likely to occur on the moons of Jupiter.

Technical information

ModeratorH2O at 316K
Incident wavelength range~0.15 to ~5.4 Å (peak flux at ~0.9 Å)
Incident flight path14.0 m
Incident beam dimensions (max)40 mm (h) x 15 mm (w)
Detector solid angle5.67 ster (coverage from 6.7° - 167° 2θ)
Typical sample volume0.5 - 1 cm3 (but can be as small as ~10 mm3)

Related resources

Sample environment

Typical sample environment equipment:

  • Room temperature sample changer (20 positions)
  • Furnace (room temperature to 1000°C)
  • Pulse Tube CCR (5 K to 300 K)
  • Helium flow cryostat (2 K to 300 K)
    Accepts dilution insert to reach ~0.1 K using copper IVC and sample can.

Visit the ISIS sample environment page or speak to your instrument contact.

Software

  • Mantid for data reduction (normalisation and generation of data files for, e.g. GSAS, GSAS-2, Topas, Fullprof).
  • Gudrun for total scattering data analysis.

Recent publications

Instrument reference

All publications and datasets based on experiments using Polaris should cite that the data is collected by DOI: 10.5286/isis.instrument.3713. Experiment DOIs follow the format 10.5286/ISIS.E.RBXXXXXXX, where XXXXXXX is the 7-digit experiment (RB) number and these can be viewed via the Data Gateway.

Reference publication: R.I. Smith, S. Hull, M.G. Tucker, H.Y. Playford, D.J. McPhail, S.P. Waller and S. T. Norberg, “The upgraded Polaris powder diffractometer at the ISIS neutron source,” Rev. Sci. Instrum. 90, 115101 (2019). DOI: 10.1063/1.5099568